Synchrotron Radiation Techniques In Industrial Chemical And Materials Science

The individual papers that comprise this monograph are derived from two American Chemical Society (ACS) Fall National Meetings that focused on the current uses of synchrotron radiation (SR) research techniques. The first Symposium was held in Washington, DC, in August 1994, and the second convened in Chicago, IL, in August 1995. The intent of these symposia was to present a broad overview of several current topics in industrial, chemical, and materials-based SR research to a chemically inclined audience. The SR techniques covered were divided roughly into the three general fields of industrial, chemical, and materials science for this purpose. Included within these four categories are environmental, geologic, atomic/molecular, analytical, solid state physics, surface science, and biological applications of SR. There is little doubt that structural biology and environmental science are the largest growth areas in SR research as this monograph goes to press. The spirit of these symposia was to bring together the expert synchrotron radiation user with new and potential users of SR techniques. There are now a preponderance of particle storage rings, located throughout the world, devoted exclusively to the production of SR. There have been great improvements in the particle accelerators and storage rings from which SR emanates. These newest third generation SR sources are the result of the successful collaboration between SR users and accelerator physicists which has made a reality out of experiments never before possible.

Meeting the long-felt need for in-depth information on one of the most advanced material characterization methods, a top team of editors and authors from highly prestigious facilities and institutions covers a range of synchrotron techniques that have proven useful for materials research. Following an introduction to synchrotron radiation and its sources, the second part goes on to describe the various techniques that benefit from this especially bright light, including X-ray absorption, diffraction, scattering, imaging, and lithography. The thrid and final part provides an overview of the applications of synchrotron radiation in materials science. bridging the gap between specialists in synchrotron research and material scientists, this is a unique and indispensable resource for academic and industrial researchers alike.

Besides its coverage of the four important aspects of synchrotron sources, materials and material processes, measuring techniques, and applications, this ready reference presents both important method types: diffraction and tomography. Following an introduction, a general section leads on to methods, while further sections are devoted to emerging methods and industrial applications. In this way, the text provides new users of large-scale facilities with easy access to an understanding of both the methods and opportunities offered by different sources and instruments.

Synchroton radiation (SR) is utilized in most scientific fields. This book will therefore be useful not only for researchers engaged in analytical chemistry, and those studying the basic fields such as physics, chemistry, biology, as well as earth science, medicine, and life science but also for those engaged in research for elucidating structure of material and its function in the application fields including applied physics, semiconductor engineering, and metal engineering. The book has a highly interdisciplinary character. The outstanding characteristics of SR have also contributed to the rapid development of new fields and applications in analytical chemistry. Features of this book: • Explains the basics of SR • Facilities and instrumentation are covered to facilitate the planning of experiments using SR. • Aspects for the future development of SR are included together with an introduction to the latest techniques which are expected to find increasing use in the coming years. This book should stimulate students specializing in analytical chemistry and materials science to have an interest in SR. In addition, it will provide scientists who are beginning analytical chemistry research using SR with instructive and illustrative descriptions. The book can also be used as an explanatory text for advanced research on the application of SR.

The 57 papers update the status of characterization techniques that use synchrotron radiation since the previous symposium on the subject in the spring of 1996. The techniques considered include X-ray absorption and scattering, imaging, tomography, microscopy, and topographic methods. Among the materials are surfaces, interfaces, electronic materials, metal oxides, solar cells, thin films, carbides, polymers, alloys, nanoparticles, and graphitic materials. Some of the papers are doubled spaced. Annotation copyrighted by Book News, Inc., Portland, OR

This book introduces the reader to the basic concepts of the generation and manipulation of synchrotron light, its interaction with matter, and the application of synchrotron light in the “classical” techniques, while including some of the most modern technological developments. As much as possible, complicated mathematical derivations and formulas are avoided. A more heuristic approach is adopted, whereby the general physical reasoning behind the equations is highlighted. Key features: A general introduction to synchrotron radiation and experimental techniques using synchrotron radiation Contains many detailed “worked examples” from the literature Of interest for a broad audience - synchrotrons are possibly one of the best examples of multidisciplinary research Four-colour presentation throughout

This conference brings together leading edge researchers from around the world and is a celebration of the increasingly important relationship between materials science and synchrotron radiation research. Special attention was given to the contribution that Synchrotron Radiation techniques have given to unsolved problems in Materials Science. The main organizer of SRMS-6 was the Brazilian Synchrotron Laboratory, with support from several Brazilian and Latin-American Agencies and Universities. The main topical areas of this conference series are, Archaeological Materials, Catalysts and clusters, Complex oxides, Data-storage and Engineering materials, Films, Surfaces and Interfaces, Geo-physical and Electronic materials, Glasses and Ceramics, Liquids, Magnetism, Materials under Extreme conditions (high pressure, etc.), Metals and Alloys, Metamaterials, Molecular electronics, Multiferroics, Nanostructured materials and Self-assembly, Polymers and Biomaterials, Photo materials, Nanofocus techniques, Strongly correlated materials, Superconducting materials, Industrial use of SR, Instrumentation/Recent Developments.

Besides its coverage of the four important aspects of synchrotron sources, materials and material processes, measuring techniques, and applications, this ready reference presents both important method types: diffraction and tomography. Following an introduction, a general section leads on to methods, while further sections are devoted to emerging methods and industrial applications. In this way, the text provides new users of large-scale facilities with easy access to an understanding of both the methods and opportunities offered by different sources and instruments.

Much like earlier books in the series, this collection of papers, first published in 2001, brings together the materials science community and the characterization techniques that use synchrotron radiation. Surfaces, interfaces, electronic materials, thin films, carbides, polymers and alloys are all addressed. And while the editors did not anticipate that the cluster of papers treating cementitious materials would necessitate a separate section, it is interesting to see the application of cutting-edge techniques to Portland cement, a very complex materials system long used in engineering structures. Topics include: X-ray diffraction - structures and transformations; X-ray diffraction - stress, strain and texture; microtomography and microdiffraction; SR methods applied to cementitious materials; magnetic materials; X-ray absorption and photoemission; and X-ray scattering and interfaces.

Synchrotron radiation is today extensively used for fundamental and applied research in many different fields of science. Its exceptional characteristics in terms of intensity, brilliance, spectral range, time structure and now also coherence pushed many experimental techniques to previously un-reachable limits, enabling the performance of experiments unbelievable only few years ago. The book gives an up-to-date overview of synchrotron radiation research today with a view to the future, starting from its generation and sources, its interaction with matter, illustrating the main experimental technique employed and provides an overview of the main fields of research in which new and innovative results are obtained. The book is addressed to PhD students and young researchers to provide both an introductory and a rather deep knowledge of the field. It will also be helpful to experienced researcher who want to approach the field in a professional way.